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Naturforsch. 1998, 53b, 720. Arduengo, A. ; Calabrese, J. C. J. Am. Chem. Soc. 1994, 116, 3625. ; Henkel, G. J. Chem. , Chem. Commun. 1993, 1778. Trotter, J. ; Wiley: Chichester, 1973, part 1, p. 49. Arduengo, A. ; Calabrese, J. ; Davidson, F. J. Am. Chem. Soc. 1991, 113, 9704. Arduengo, A. ; Calabrese, J. ; Marshall, W. J. Chem. Lett. 1999, 1021. Arduengo, A. ; Marshall, W. J. Z. Anorg. Allg. Chem. 1999, 625, 1813. ADVANCES IN INORGANIC CHEMISTRY, VOL. 50 GROUP I COMPLEXES OF P- AND As-DONOR LIGANDS KEITH IZOD Department of Chemistry, University of Newcastle, Newcastle upon Tyne, United Kingdom, NE1 7RU I.
However, heating a toluene solution to 90ЊC results in LiF elimination to generate the ﬁve-membered heterocycle 19. The lithium complex with R ϭ Me undergoes a different decomposition process and yields the four-membered heterocycle 20 on heating to 90ЊC, via Li–F elimination. Several boryl-substituted lithium phosphides, [Li͕PRB(Ar)2͖Ln] [Ar ϭ mes, R ϭ Cy, Mes, 1-adamantyl, Ln ϭ (OEt2)2 ; Ar ϭ mes, R ϭ SiMe3 , GROUP I COMPLEXES OF P- AND As-DONOR LIGANDS 49 SCHEME 2. Reactions of [Li͕P[SiF(Is)2][P(NR2)2]͖(THF)](R ϭ Pri, Me).
Tetrahedron Lett. 1997, 38, 2501. For a review of terminal chalcogenido complexes, see Kuchta, M. ; Parkin, G. Coord. Chem. Rev. 1998, 176, 323. 32 57. 58. 59. 60. 61. 62. 63. 64. 65. 66. 67. 68. 69. 70. 71. 72. 73. ; Kratz, T. Chem. Ber. 1993, 126, 2047. Arduengo, A. , III; Burgess, E. M. J. Am. Chem. Soc. 1976, 98, 5020. Arduengo, A. , III; Burgess, E. M. J. Am. Chem. Soc. 1977, 99, 2376. Janulis, E. ; Arduengo, A. , III. J. Am. Chem. Soc. 1983, 105, 3536. Arduengo, A. , III; Burgess, E. M. J.